千年健挥发油微波辅助提取研究
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Microwave-assisted solvent extraction of essential oils from Homalomena Occulta
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    摘要:

    采用微波辅助溶剂萃取法(MASE)提取千年健挥发油,并利用GC-MS技术对其化学成分进行了分析。最佳条件为石油醚作溶剂,微波功率600W,60℃下提取25min。共鉴定出63种成分,主要为芳樟醇(23.411%),7-乙酰基-2-羟基-2-甲基-5-异丙基二环[4,3,0]壬烷(5.222%),4-松油醇(3.971%)。与传统水蒸气蒸馏法(HD)比较发现,MASE法节省时间,得率更高,同时化学组成成分差异不大,是一种完全可以替代HD法提取千年健挥发油的高效、节能的提取技术。

    Abstract:

    Microwave-assisted solvent extraction (MASE) essential oils from Homalomena Occulta. The chemical composition of the oil was identified using GC/MS technique. The optimum conditions are obtained: petroleum ether as solvent, the microwave power 600W, extraction temperature 60℃, extraction time 25min. 63 constituents were identified total and The main chemical constituents were Linalool (23.411%), 7-Acetyl-2-hydroxy-2-methyl -5- isopropylbicyclo[4.3.0]nonane (5.222%), 4-Terpineol (3.971 %). Comparison with the conventional hydro-distillation (HD), it was found that MASE save time and higher yield but no significant differences of the chemical composition. Therefore, MASE was a complete substitute for HD, high efficiency and energy savings technology.

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余汉谋,肖海鸿,姜兴涛,傅国锋,杨文彬,吴苑存,强耀锋.千年健挥发油微波辅助提取研究[J].精细化工,2011,28(12):

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  • 收稿日期:2011-08-17
  • 最后修改日期:2011-10-21
  • 录用日期:2011-11-01
  • 在线发布日期: 2011-12-09
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