AEDA/GC-MS分析新鲜芫荽香气成分
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TS207.3

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国家重点研发计划(2016YFD0400705);国家自然科学基金青年基金项目(31401604)


Analysis of Aroma Compounds in Coriander by GC-MS and AEDA
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National Key R&D Program(2016YFD0400705);Supported by the National Natural Science Foundation of China (31401604).

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    摘要:

    采用溶剂辅助风味蒸发法(SAFE)结合气相色谱-质谱联机(GC-MS),通过双柱对新鲜芫荽中的挥发性成分进行鉴定,并通过谱库检索和保留指数比对,共计从新鲜芫荽中鉴定出化合物87种,其中烃类28种,醛类20种,醇类22种,酸类4种,酯类7种,酮类3种,杂环及其他类3种。通过香气提取物稀释分析法 (AEDA) 结合气相色谱-嗅闻技术(GC-O)对新鲜芫荽进行分析,共鉴定出21种活性香气成分,其中关键香气的物质有5种 (FD≥81),分别是反-2-十二烯醛、反-2-十三烯醛、反-2-十四烯醛、3-甲硫基丙醛、反-2-癸烯醛。

    Abstract:

    Volatile compounds of the fresh coriander were analyzed by solvent-assisted flavor evaporation (SAFE) and gas chromatography-mass spectrometry (GC-MS). By NIST 11 Mass Spectral Library searching and retention index comparison, a total of 87 compounds were identified, including 28 hydrocarbons, 20 aldehydes, 22 alcohols, 4 organic acid, 7 esters, 3 ketones, 3 amines and others. GC-O combined with aroma extract dilution analysis(AEDA) was applied to identify aroma active compounds in the fresh coriander , and 21 aroma compounds were identified. 5 chemicals were identified as key aroma compounds (FD≥81), namely trans-2-dodecenal, trans-2-tridecenal, trans-2-tetradecenal, methional and trans-2-decenal.

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马明娟,王丹,谢恬,陈海涛,孙宝国,张玉玉. AEDA/GC-MS分析新鲜芫荽香气成分[J].精细化工,2017,34(8):

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  • 收稿日期:2017-05-05
  • 最后修改日期:2017-06-22
  • 录用日期:2017-07-10
  • 在线发布日期: 2020-03-23
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