According to the structure rules of sandalwood compounds, 3-terpenylcyclohexanol was prepared. 3-terpenylcyclohexanol was synthesized from 3-bromophenol via protection reaction、Grignard reaction and hydronation. The total yield of the three steps was 44% and the ratio of trans/cis was about 1:1. The product had moody, floral with sandalwood flavor. The novelty of this research was testified by the Mininstry of Education Novelty Search Workstations (L06) on June 27, 2008. The testified number was L06-080103.