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·1296· 精细化工 FINE CHEMICALS 第 37 卷
(2)荧光性能测试和 TGA 测试结果显示, 1(10): 55-59.
4
AC-DETA-2PA 的荧光强度达到 4.08×10 ,具有优良 [11] LIDIA M L, PAULO C, ALEXANDRE L M, et al. Synthesis and
的荧光性质,在光学应用方面具有潜在价值。 anti-inflammatory activity of phthalimide derivatives, designed as
new thalidomide analogues[J]. Bioorganic and Medicinal Chemistry,
AC-DETA-2PA 的耐热温度为 275 ℃,表明化合物具
2012, 10(9): 3067-3073.
有良好的热稳定性,有望能用于荧光耐热材料方面。 [12] SAMIRA M, MENANA E H, KHALID D. 3D-QSAR for α-glucosidase
(3)AC-DETA-2PA 的最佳合成工艺条件为: inhibitory activity of N-(phenoxyalkyl) phthalimide derivatives[J].
反应时间 4 h,n(AC)∶n(DETA-2PA)=1.6∶1.0,反 International Journal of Recent Research and Applied Studies, 2012,
应温度 25 ℃,催化剂氢化钠用量占反应物总质量 11(3): 395-401.
[13] OKUNROBO L O, USIFOH C O, SCRIBA G K E. Synthesis and
的 8.46%。在此工艺条件下,AC-DETA-2PA 胺值为
pharmacological evaluation of 2-hydroxy methyl benzamides as
2.96 mg KOH/g。此后研究应着重于 AC-DETA-2PA
antiinflammatory and analgesic agents[J]. Acta Poloniae Pharmaceutica,
的提纯和利用其活性双键基团合成新的中间体,拓 2006, 63: 25-31.
宽邻苯二甲酰亚胺类化合物的种类,提供更丰富的 [14] YANG H K (杨海葵), XU W F (许万福), DUAN A N (段安娜), et
应用。 al. Synthesis and biological activity of imine and imide compounds
containing 1,2,4-triazole rings[J]. Chemical Journal of Chinese
参考文献: Universities (高等学校化学学报), 2014, 35(3): 555-563.
[15] FIRSTOVA A A, KOFANOV E R, ZAKSHEVSKAYA V M, et al.
[1] JIA H Z (贾会珍), ZHANG P (张萍), SUN Y R (孙耀冉), et al.
Synthesis of amides of carboxylic acids with an imide and alicyclic
Synthesis of carboxyl functionalized imide derivatives by the direct
fragments and a study of their genotoxic activity in the allium test[J].
reaction of aminoacids with anhydrides [J]. China Journal of Organic
Russian Journal of Bioorganic Chemistry, 2019, 45(3): 204-213.
Chemistry (有机化学), 2006, 26(1): 99-102.
[16] GAO X H (高旭红), LI B Q (李炳奇). Amino protection and
[2] TOMOMI N, HIROYUKI M, RVOHEI K, et al. Cell differentiation
application in organic synthesis (review)[J]. Journal of Shihezi
inducers derived from thalidomide[J]. Bioorganic and Medicinal
University (Natural Science Edition) (石河子大学学报:自然科学
Chemistry Letters, 2005, 15(13): 3212-3215.
版), 1999, 3(1): 76-86.
[3] YOSUVA S M, SABASTIYAN A. Synthesis, characterization and
[17] HUANG Y F (黄月芳). Synthesis of dipeptide and glucose peptide by
antimicrobial activity of cobalt (Ⅱ) and nickel (Ⅱ) complexes with a
novel mannich base 2-(diethylaminomethyl)isoindoline-1,3-dione [J]. phthalic anhydride method[D]. Nanjing: Nanjing Agricultural University
International Journal of ChemTech Research, 2012, 4: 805-815. (南京农业大学), 2008.
[4] SHARMA U, KUMAR P, KUMAR N, et al. Recentadvances in the [18] WANG T G (王庭钢), LI X (李鑫), WU F (吴芳), et al. Synthesis of
chemistry of phthalimide analogues and their therapeutic potential[J]. phthalimide and N-hydroxymethylphthalimide[J]. Shandong
Mini Review in Medicinal Chemistry, 2010, 10(8): 678-704. Chemical Industry (山东化工), 2017, 46(17): 1-3.
[5] SRINIVASAN R, KUMAR K R, KUMAR P. Synthesis and [19] YANG H H (杨欢欢), GUO Z Q (郭振强), WANG J (王筠).
antimicrobial activity of some new α N-phthilimido aminoacids Synthesis of phthalimide besylate[J]. Zhejiang Chemical Industry (浙
analogues[J]. International Journal of ChemTech Research, 2010, 2: 江化工), 2015, 46(7): 40-41.
895-898. [20] DENG F (邓丰). Synthesis of N,N′-ethylenebistetrabromophthalimide [D].
[6] EVYAPAN M, CAPAN R, NAMLI H, et al. Formation of Nanjing: Nanjing University of Science and Technology (南京理工
Langmuir-Blodgett thin film of a novel N-dodecyl phthalimide[J]. 大学), 2007.
Material Letters, 2006, 60(19): 2371-2374. [21] LI J (李建), LIU Y L (刘裕立), LI Q J (李强军), et al. Preparation of
[7] WINTER G E, BUCKLEY D, PAULK J, et al. Drug development. N-(2-hydroxyethyl)-phthalimide by Gabriel synthesis[J]. Fine Chemical
phthalimide conjugation as a strategy for in vivo targetprotein Intermediates (精细化工中间体), 2004, 34(4): 31-32.
degradation[J]. Science, 2015, 348(6241): 1376-1381. [22] ZHANG L L (张丽丽), SHEN J (沈军), GANGBEN J N (岡本佳男),
[8] WANG Q H (王庆华), WENG W (翁文), LAN L J (兰丽娟), et al. et al. Preparation and chiral recognition ability of 2-N-phthalimide
Synthesis and optical properties of phthalimide amide chiral molecular chitosan-based chiral stationary phase[J]. Acta Polymerica Sinica (高
clamps[J]. Chinese Journal of Synthetic Chemistry (合成化学), 分子学报), 2016, (11): 1555-1562.
2009, 17(5): 583-585, 602. [23] WU Y Y (伍媛媛), SHAO Y D (邵艳东), LI D X (李冬雪), et al.
[9] MACHADO A L, LIMA L M, ARAUJO J X, et al. Design, synthesis Study on the synthesis conditions of N-(2-chloroethyl) phthalimide[J].
and antiinflammatory activity of novel phthalimide derivatives, Fine Chemical Intermediates (精细化工中间体), 2013, 43(6): 56-58.
structurally related to thalidomide[J]. Bioorg Med Chem Lett, 2005, [24] MAO Q (茅琦), NI H Q (倪惠琼). Synthesis of N-acryloylphthalimide[J].
15(4): 1169-1172. Applied Chemical Industry (应用化工), 2013, 42(12): 2246-2248.
[10] VEENA K, PATHAK P. Synthesis and anticonvulsant activity of [25] YE M J (叶美君). Determination of amine value in polyamide
some N-substituted-phthalimide analogs[J]. Pharma Innovation, 2012, resin[J]. Thermosetting Resin (热固性树脂), 1999, 14(2): 51-53.