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·344·                             精细化工   FINE CHEMICALS                                  第 37 卷

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               图 5   不同提取方法所制油茶籽油判别因子分析图                           Chimica Acta, 2002, 459(2): 219-228.
            Fig. 5    Discriminant factor  analysis of  Camellia  oleifera   [8]   Mildner-szkudlarz S, Jelen H H. Detection of olive oil adulteration
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                (1)通过对不同提取方法制备油茶籽油出油率                          [10]  Jiang Jinjin (江津津), Chen Lihua (陈丽花), Li Haibin (黎海彬), et
            进行比较得出,冷榨法出油率最低,浸出法出油率                                 al. Flavor identification  of fish  sauce based on electronic nose[J].
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            最高,且冷榨法与其他两种方法相比具有显著性差
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            异,P<0.05,浸出法与超临界法出油率无显著性差                          [11]  National Health and Family Planning Commission  of the People's
            异,P>0.05。由于浸出法制备油茶籽油的成本较低                              Republic of China (中华人民共和国国家卫生和计划生育委员会).
                                                                   GB 5009. 229—2016: National food safety standards—Determination
            且其出油率较高,所以市场经济效益比其他两种方                                 of acid value in foods [S]. Beijing: Standards Press of China (中国标
            法高。                                                    准出版社), 2016: 1-20.
                                                               [12]  Standardization Administration of the People's Republic of China (中
                (2)通过对不同提取方法所制油茶籽油进行客
                                                                   国国家 标准 化管 理委员 会 ). GB/T 5534—2008: Animal and
            观品质分析比较可知,3 种油茶籽油品质存在差异,                               vegetable fats and  oils—Determination of saponification value [S].
            超临界法所制油茶籽油的酸价、碘值与过氧化值均                                 Beijing: Standards Press of China (中国标准出版社), 2008: 1-12.
                                                               [13]  Standardization Administration of the People's Republic of China (中
            小于其他两种方法,并且其过氧化值与其他两种油                                 国国家 标准 化管 理委员 会 ). GB/T 5532—2008: Animal and
            茶籽油具有显著性差异,P<0.05;3 种油茶籽油的                             vegetable fats and oils—Determination of iodine value [S]. Beijing:
                                                                   Standards Press of China (中国标准出版社), 2008: 1-12.
            中性色泽指标均具有显著性差异,P<0.05,冷榨法
                                                               [14]  National Health and Family Planning Commission  of the People's
            最低,浸出法最高;3 种油茶籽油的皂化值并无显                                Republic of China (中华人民共和国国家卫生和计划生育委员会).
            著性差异,P>0.05,浸出法最低,冷榨法最高;3                              GB 5009. 227—2016: National food safety standards—Determination
                                                                   of peroxide values in foods[S]. Beijing: Standards Press of China (中
            种油茶籽油脂肪酸组成具有一定差异。不同提取方                                 国标准出版社), 2016: 1-12.
            法能够对油茶籽油品质产生影响。                                    [15]  National Health and Family Planning Commission  of the People's
                                                                   Republic of China (中华人民共和国国家卫生和计划生育委员会).
                (3)电子鼻技术的主成分分析法中,主成分累
                                                                   GB 5009. 236—2016: National food safety standards—Determination
            计方差贡献率为 99.622%,判别因子分析法中,主                             of moisture and volatile matter of animal and vegetable oils and fats
            成分累计方差贡献率为 99.999%,DI 均为 88,电子                         [S]. Beijing: Standards Press of China (中国标准出版社), 2016: 1-8.
                                                               [16]  Standardization Administration of the People's Republic of China (中
            鼻技术能够对不同提取方法所制油茶籽油进行有效                                 国国家标准化管理委员会). GB/T 22460—2008: Animal and
            区分。通过这种方法,能够实现判别市售油茶籽油                                 vegetable fats and oils—Determination of Lovibond colour [S].
                                                                   Beijing: Standards Press of China (中国标准出版社), 2008: 1-12.
            提取方法的目的。                                           [17]  Standardization Administration of the People's Republic of China (中
                                                                   国国家标准化管理委员会). GB/T 5525—2008: Vegetable fats and
            参考文献:                                                  oils—Method for identification of transparency, odor and flavor [S].
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