Page 61 - 精细化工2019年第8期
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第 8 期                        王   琛,等: PBF 的合成及其复合材料的光/热固化                               ·1549·


            3   结论                                                 Science, Polymer Edition, 2009, 20(1): 49-69.
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                                1
                (1)通过 FTIR、 HNMR 及 GPC 等表征,证明                      Preparation and curing properties of iniectable PPF bone cement[J].
            成功合成聚富马酸丁二醇酯。其较佳的合成工艺条                                 Journal  of  Functional  Polymers  (功能高分子学报),  2018,  31(1):
            件为:反应温度 130  ℃,反应时间 8 h,n(富马酸                          51-56.
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            二乙酯)∶n(1,4-丁二醇)=1∶3,且在此条件下
                                                                   encapsulation  of  polymer  composites  based  on  poly(propylene
            产率为 61.94%。
                                                                   fumarate)  crosslinked  with  poly(propylene  fumarate)-diacrylate[J].
                (2)在紫外光源与试样的距离为 5 cm、波长为                           RSC Adv, 2015, 5(65): 52888-52895.
            200~450  nm、紫外光辐照时间为 2  min 的条件下,                  [9]   Chen Jingmin (陈靖民), Hua Fengjun (华峰君), Qiu Jiang (邱江), et
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                (3)在恒温环境下,热固化分析结果显示,当                              Spectroscopy  and  Spectral  Analysis  (光谱学与光谱分析),  2001,
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            BPO 质量分数为 3%(促进剂 DMT质量分数为 0.2%)
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            时,交联固化效果最佳。
                                                                   the  influence  of  external  heating  on  dental  composite
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            料领域应用奠定了基础。                                            diacrylate macromers as crosslinking agents and characterization of
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