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第 9 期                  李维新,等:  超微粉碎-微波双水相萃取红花龙胆中环烯醚萜苷类                                  ·1839·


            DPPH·清除能力逐渐增强,但对 DPPH·清除能力强                        [3]   Wu Lihong (吴立宏), Guan Haifeng (官海峰), Yu Li (俞丽), et al.
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            弱不一,在 0.2~1.0 g/L 内,微波辅助双水相红花龙                         Minzu University of China Natural Science Edition (中央民族大学
            胆全草提取液对 DPPH·清除能力明显比 BHT 强但                            学报:  自然科学版), 2011, 20(2): 76-80.
                                                               [4]   Yang  Weixia  (杨维霞),  Zhao  Le  (周乐),  Geng  Huilin  (耿会玲),  et
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            的微波控温辅助双水相提取最佳工艺条件为:在                              [7]   Ratanapongleka K. Recovery of biological products in aqueous two
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            体系中,干粉粒度 400 目,微波温度(70±1)℃,                            New York: Wiley, 1986.
            微波时间 110 s,红花龙胆干粉加入量 3.5 g。在此工                     [9]   Federico R R, Jorge B, Oscar A, et al. Aqueous two-phase affinity
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            达到 5.48%。                                          [10]  Wang Jianhong (汪建红), Liao Limin (廖立敏), Wang Bi (王碧), et
                 红花龙胆全草中环烯醚萜苷类的抗氧化能力在                              al.  Extraction  of  limonin  in  lemon  peel  by  ultrasonic-assisted
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            0.2~0.6 g/L 内比 BHT 强,对 DPPH 自由基的清除能
                                                                   Development (天然产物研究与开发), 2015, 27(6): 1081-1085.
            力在 0.2~1.0  g/L 内比 BHT 强。下一步将对其体内                  [11]  Huang Qichun (黄其春), Lin Meixiang (林梅香), Hong Yanping (洪
            抗氧化活性等生物学特性进行深入研究,从活性成                                 燕萍), et al. Effect of ultrafine grinding on the dissolution of total
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            分的生物转化角度阐述环烯醚萜苷类的利用机理,                                 Sciences (安徽农业科学), 2012, 40(10): 5884-5885, 5917.
            提高其活性成分利用,使其药用价值产生更大的经                             [12]  Cao  Yuan  (曹渊),  Li  Chuangju  (李创举), Xia Zhining (夏之宁).
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            粉进行萃取,并进行 HPLC 分析检测。与文献中传                              2857-2858.
            统的检测方法相比,此法不用通过富集等分离纯化                             [13]  Yu  Huanhuan  (喻欢欢),  Ji  Guangjianzhidai  (吉光见稚代),  Xu
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            溶出环烯醚萜苷发生聚合反应的几率,实现了红花                                 glucosidase  activity  in  Radix  Scrophulariae[J].  Chinese  Journal of
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            使用不同粉碎工艺提取环烯醚萜苷类,发现超微粉                             [14]  Cheng Yupeng (程玉鹏), Ma Aiping (马爱萍), Chen Qi (陈琦), et al.
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            小均匀,增加了比表面积,有利于环烯醚萜苷类的                             [15]  Benzie I F, Strain J J. The ferric reducing ability of plasma(FRAP) as
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            碎成本和杂质浸出率,所以要综合考虑是否适合于
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