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第 12 期                   艾绿叶,等:  响应面优化烟叶多糖磷酸化工艺及保润性评价                                   ·2071·


            粗多糖经过醇析、洗脱等步骤,得到提取率为 3.18%                         [11]  Tao Tao (陶陶),  He Fan (贺凡), Ji Xiaoming (姬小明),  et al.
                                                                   Response surface methodology for  optimization  of flash  extraction
            的烟叶多糖。Box-Behnken 法制备磷酸化烟叶多糖
                                                                   for fenugreek  (trigonella foenum-graecum L.) polysaccharides and
            的最佳工艺条件为:反应时间 6.1 h、pH=9.0,反应                          research of its humectant properties[J]. Fine Chemicals (精细化工),
            温度 95  ℃,此条件下,磷酸化烟叶多糖的磷酸根                              2016, 33(6): 666-673.
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            质量分数达到 11.68%。                                         al. Ultrasonic extraction technique for polysaccharide from wedelia
                 (2)采用差量法测量添加磷酸化烟叶多糖、烟                             prostrate and moisture retentivity of polysaccharide in cigarettes[J].
            叶多糖、丙二醇和蒸馏水的烟丝含水率,持水效果                                 Tobacco Science & Technology (烟草科技), 2014, (2): 44-48.
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            为:磷酸化烟叶多糖>烟叶多糖>丙二醇>蒸馏水。                                Chemical modification of levan from Bacillus amyloliquefaciens and
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            磷酸化烟叶多糖的评吸结果优于烟叶多糖,且当添
                                                                   100.
            加量为烟丝质量的 0.05%~0.1%时,能有效改善卷烟                       [14]  Chen Y, Zhang H, Wang Y, et al. Acetylation and carboxymethylation
            吸食品质。推测可能的原因是引入的磷酸基团改变                                 of the polysaccharide from Ganoderma atrum  and their antioxidant
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            了烟叶多糖的理化性质,导致磷酸化烟叶多糖在持                                 279-288.
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